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We are a participant in the Amazon Services LLC Associates Program, an affiliate advertising program designed to provide a means for us to earn fees by linking to Amazon.com and affiliated sites. File only crack windows xp sp 3.Microwave assisted hydrothermal synthesis, characterization and catalytic application of nano-layered nickel sulphide for simultaneous removal of Cr(VI) and As(V) from aqueous solution.

Nano-layered nickel sulphide was synthesized using microwave assisted hydrothermal process. The prepared nickel sulphide nanoparticles were characterized using X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM) and energy dispersive X-ray spectroscopy (EDS). The prepared nickel sulphide has a porous and mesoporous morphology with the size ranging from 50 to 150 nm. The XRD patterns indicate that the nickel sulphide nanostructures prepared have a cubic phase structure. The crystallite size of the nickel sulphide was found to be 38 nm by using Debye-Scherrer's formula. The Fourier transform infrared (FTIR) analysis indicates the presence of -OH and -SO3 groups on the surface of nickel sulphide. The nickel sulphide nanostructures have a high surface area value of 52.33 m2/g. The surface area was further improved by grafting of amorphous carbon (AC) using chemical vapour deposition technique. The catalytic efficiency of the synthesized nanoparticles was tested for simultaneous removal of Cr(VI) and As(V) from aqueous solution. The percentage of Cr(VI) and As(V) removal were found to be 96.56% and 92.58% within 5 min of reaction time, respectively. The process was found to be pH dependent and the effect of initial Cr(VI) concentration on the removal efficiency was also studied. The kinetics of removal of Cr(VI) and As(V) from aqueous solution was also studied. The removal of Cr(VI) and As(V) follows pseudo-second order kinetics. The surface functional groups present on the nanoparticles were investigated using Fourier transform infrared (FTIR) and 0b46394aab

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